Huadai Chemical
PRODUCTS
Diethyl Oxalate
Huadai Chemical
|
HS Code |
202900 |
| Name | Diethyl Oxalate |
| Chemical Formula | C6H10O4 |
| Molar Mass | 146.14 g/mol |
| Appearance | Colorless liquid |
| Odor | Faint, pleasant odor |
| Density | 1.0785 g/cm³ at 20 °C |
| Melting Point | -41.8 °C |
| Boiling Point | 185.4 °C |
| Solubility In Water | Slightly soluble |
| Solubility In Organic Solvents | Soluble in ethanol, ether, benzene, etc. |
| Flash Point | 75 °C (closed cup) |
| Vapor Pressure | 0.13 kPa at 20 °C |
As an accredited Diethyl Oxalate factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.
| Packing | Diethyl Oxalate in 25 - kg drum packaging for secure storage and transport. |
| Storage | Diethyl oxalate should be stored in a cool, well - ventilated area, away from heat sources and ignition points due to its flammability. Keep it in a tightly sealed container to prevent vapor release. Store it separately from oxidizing agents and strong acids as it can react with them. Regularly check storage conditions to ensure safety. |
| Shipping | Diethyl Oxalate is shipped in tightly - sealed, corrosion - resistant containers. Transport must comply with hazardous chemical regulations, ensuring proper labeling, secure packaging to prevent leakage during transit. |
Competitive Diethyl Oxalate prices that fit your budget—flexible terms and customized quotes for every order.
For samples, pricing, or more information, please call us at +8615371019725 or mail to sales7@bouling-chem.com.
We will respond to you as soon as possible.
Tel: +8615371019725
Email: sales7@bouling-chem.com
Historical Development
"The History of Diethyl Oxalate"
Diethyl oxalate is an important product of chemistry. At the beginning, scholars explored its properties at the end of the day. In the early years, people only knew a little about the appearance of related chemical combinations, but did not obtain the method of refining.
Catch up to later generations, chemical refinement, and the research of various sages deepened. In the process of reaction and material matching, there are detailed studies. Gradually able to control its production and increase its purity.
In the past, the production method was complex and inefficient, but now it is skillful and good, and the output has also increased sharply. It is also widely used, involving the industries of medicine and fragrances. Since the beginning of ignorance, it has become increasingly clear and rational, making good use of its properties. The development of diethyl oxalate is also a sign of the evolution of real chemistry, witnessing the process of unremitting research and technological innovation in the academic community.
Diethyl oxalate is an important product of chemistry. At the beginning, scholars explored its properties at the end of the day. In the early years, people only knew a little about the appearance of related chemical combinations, but did not obtain the method of refining.
Catch up to later generations, chemical refinement, and the research of various sages deepened. In the process of reaction and material matching, there are detailed studies. Gradually able to control its production and increase its purity.
In the past, the production method was complex and inefficient, but now it is skillful and good, and the output has also increased sharply. It is also widely used, involving the industries of medicine and fragrances. Since the beginning of ignorance, it has become increasingly clear and rational, making good use of its properties. The development of diethyl oxalate is also a sign of the evolution of real chemistry, witnessing the process of unremitting research and technological innovation in the academic community.
Product Overview
Diethyl oxalate is an organic compound. Its shape is a colorless transparent liquid with an aromatic odor. The boiling point is about 80 and 4 degrees, and the melting point is negative 40 degrees.
This substance is widely used in the field of chemical industry. In organic synthesis, it is often an important raw material. It can be used in the preparation of drugs, fragrances and pesticides. With its chemical activity, it can react with a variety of substances to obtain various useful derivatives.
The method of preparation is mostly obtained by the reaction of oxalic acid and ethanol through esterification. During the reaction, it needs to be assisted by a suitable temperature and a catalyst to promote its formation.
Diethyl oxalate plays a significant role in industrial production and scientific research, and is an indispensable material in many fields.
This substance is widely used in the field of chemical industry. In organic synthesis, it is often an important raw material. It can be used in the preparation of drugs, fragrances and pesticides. With its chemical activity, it can react with a variety of substances to obtain various useful derivatives.
The method of preparation is mostly obtained by the reaction of oxalic acid and ethanol through esterification. During the reaction, it needs to be assisted by a suitable temperature and a catalyst to promote its formation.
Diethyl oxalate plays a significant role in industrial production and scientific research, and is an indispensable material in many fields.
Physical & Chemical Properties
"Physical Properties of Diethyl Oxalate"
Diethyl oxalate is an organic compound. Its physical properties are colorless and transparent liquid, with aromatic taste. Melting point -40.6 ° C, boiling point 185.4 ° C, relative density 1.0785 (20/4 ° C), refractive index 1.4101. Insoluble in water, miscible with organic solvents such as ethanol and ether.
Its chemical properties are hydrolyzable, and gradually dissolve into oxalic acid and ethanol in case of water. It can undergo reactions such as alcoholysis and aminolysis. It interacts with bases to form oxalates and ethanol. It is an important raw material in organic synthesis and can be used to prepare drugs, fragrances, etc. Because of its specific chemical properties, it is widely used in the chemical industry.
Diethyl oxalate is an organic compound. Its physical properties are colorless and transparent liquid, with aromatic taste. Melting point -40.6 ° C, boiling point 185.4 ° C, relative density 1.0785 (20/4 ° C), refractive index 1.4101. Insoluble in water, miscible with organic solvents such as ethanol and ether.
Its chemical properties are hydrolyzable, and gradually dissolve into oxalic acid and ethanol in case of water. It can undergo reactions such as alcoholysis and aminolysis. It interacts with bases to form oxalates and ethanol. It is an important raw material in organic synthesis and can be used to prepare drugs, fragrances, etc. Because of its specific chemical properties, it is widely used in the chemical industry.
Technical Specifications & Labeling
"Technical Specifications and Labeling of Diethyl Oxalate (Commodity Parameters) "
Diethyl oxalate is one of the chemical products. Its technical specifications are related to the production method, and precise steps must be followed to ensure the best quality. The selection of raw materials must be pure; the reaction conditions, such as temperature and pressure, must be strictly controlled. In this way, good quality diethyl oxalate can be produced.
As for the label, the product parameters should be specified in detail. The name is "Diethyl Oxalate", English "Diethyl Oxalate", which cannot be wrong. Indicate the proportion of ingredients, as well as the important items related to safety and storage. If it is flammable, it should be warned on the label. Storage conditions should be dry and cool, and should also be clearly indicated. This technical specification and labeling are essential to ensure the quality and safety of diethyl oxalate.
Diethyl oxalate is one of the chemical products. Its technical specifications are related to the production method, and precise steps must be followed to ensure the best quality. The selection of raw materials must be pure; the reaction conditions, such as temperature and pressure, must be strictly controlled. In this way, good quality diethyl oxalate can be produced.
As for the label, the product parameters should be specified in detail. The name is "Diethyl Oxalate", English "Diethyl Oxalate", which cannot be wrong. Indicate the proportion of ingredients, as well as the important items related to safety and storage. If it is flammable, it should be warned on the label. Storage conditions should be dry and cool, and should also be clearly indicated. This technical specification and labeling are essential to ensure the quality and safety of diethyl oxalate.
Preparation Method
"Method of Preparation of Diethyl Oxalate"
Diethyl oxalate is also an organic compound. The method of its preparation is related to raw materials, production processes, reaction steps and catalytic mechanisms.
The raw materials are often based on ethanol and oxalic acid. The ethanol and oxalic acid are placed in a reactor in a certain proportion. The production process needs to be controlled at a suitable temperature, preferably about 150 to 200 degrees Celsius.
The reaction steps are as follows: first mix ethanol and oxalic acid, stir well, and then gradually heat up. In the meantime, an esterification reaction occurs, and the hydroxyl group of ethanol interacts with the carboxyl group of oxalic acid.
The catalytic mechanism is also important. Sulfuric acid is often used as a catalyst to promote the reaction rate and reduce the activation energy of the reaction. In this way, after several hours of reaction, cooling and purification, the finished product of diethyl oxalate can be obtained.
Diethyl oxalate is also an organic compound. The method of its preparation is related to raw materials, production processes, reaction steps and catalytic mechanisms.
The raw materials are often based on ethanol and oxalic acid. The ethanol and oxalic acid are placed in a reactor in a certain proportion. The production process needs to be controlled at a suitable temperature, preferably about 150 to 200 degrees Celsius.
The reaction steps are as follows: first mix ethanol and oxalic acid, stir well, and then gradually heat up. In the meantime, an esterification reaction occurs, and the hydroxyl group of ethanol interacts with the carboxyl group of oxalic acid.
The catalytic mechanism is also important. Sulfuric acid is often used as a catalyst to promote the reaction rate and reduce the activation energy of the reaction. In this way, after several hours of reaction, cooling and purification, the finished product of diethyl oxalate can be obtained.
Chemical Reactions & Modifications
"Chemical Reverse Modification of Diethyl Oxalate"
Diethyl oxalate is an important substance for chemical research. Its chemical reaction is not good, but the effect is not perfect.
At the beginning of the study, its reaction is harsh, and it needs to be high, and the efficiency is not good. Its reverse theory is also unknown.
Those who think deeply about the reason, and change the product. With the new catalytic method, the effect is actually obtained. All the reactions are reduced, and the efficiency is also increased.
As for the modification, it is necessary to obtain novelty. Or add functionality to make it special.
From this, the chemical modification of diethyl oxalate is reversed, and the researchers are diligent in research, which is more beneficial, and will not be able to develop new ones.
Diethyl oxalate is an important substance for chemical research. Its chemical reaction is not good, but the effect is not perfect.
At the beginning of the study, its reaction is harsh, and it needs to be high, and the efficiency is not good. Its reverse theory is also unknown.
Those who think deeply about the reason, and change the product. With the new catalytic method, the effect is actually obtained. All the reactions are reduced, and the efficiency is also increased.
As for the modification, it is necessary to obtain novelty. Or add functionality to make it special.
From this, the chemical modification of diethyl oxalate is reversed, and the researchers are diligent in research, which is more beneficial, and will not be able to develop new ones.
Synonyms & Product Names
"The same name and trade name of diethyl oxalate"
Diethyl oxalate, there are many people with the same name, and the world has different names. In the field of chemical industry, or diethyl oxalate, this is named according to its chemical composition, which precisely indicates the molecular structure. There are also people who call it ethyl oxalate, although simple but without losing the essence, all refer to this thing.
Its trade names are also rich and diverse. Merchants give it a unique name in recognition of its characteristics and in response to the needs of the market. For example, "crystal pure diethyl oxalate" highlights the high purity of the product, seems to be crystal clear, and has high quality to attract buyers' eyes. Another example is "excellent grade diethyl oxalate", which shows its excellent quality and is outstanding among all its kind. This equivalent name and trade name are both logos for chemical exchanges and business exchanges, helping industry operators to identify and make products their own.
Diethyl oxalate, there are many people with the same name, and the world has different names. In the field of chemical industry, or diethyl oxalate, this is named according to its chemical composition, which precisely indicates the molecular structure. There are also people who call it ethyl oxalate, although simple but without losing the essence, all refer to this thing.
Its trade names are also rich and diverse. Merchants give it a unique name in recognition of its characteristics and in response to the needs of the market. For example, "crystal pure diethyl oxalate" highlights the high purity of the product, seems to be crystal clear, and has high quality to attract buyers' eyes. Another example is "excellent grade diethyl oxalate", which shows its excellent quality and is outstanding among all its kind. This equivalent name and trade name are both logos for chemical exchanges and business exchanges, helping industry operators to identify and make products their own.
Safety & Operational Standards
"Code for the safe production and operation of diethyl oxalate"
Diethyl oxalate is one of the chemical products. To make this product, it is necessary to clarify its safety and operation specifications, so that it can be smooth and safe.
In the place of production, the first priority is safety. All facilities in the factory must be sturdy and intact, and the fire, explosion-proof and anti-virus equipment should be complete. When workers are working, they must wear special protective clothing, gas masks, goggles, etc., to prevent harm from contact with this product. In the workshop, ventilation must be good so that harmful gases can be discharged in time.
Its operation is also regulated. When feeding, the proportion and order of materials should not be wrong, and it should be done according to the precise formula. When reacting, the temperature and pressure must be strictly controlled, and a special person should be set up to monitor the number of instruments. If there is any abnormal movement, it should be disposed of immediately. The process of heating and cooling should also be done slowly and cannot be done.
Store diethyl oxalate, and also pay attention to it. It should be placed in a cool, dry and ventilated place, away from fire and heat sources. Do not mix with oxidants, acids and other substances to prevent chemical reactions and cause danger.
When handling, the action should be gentle, and it should not be loaded and unloaded savagely to avoid leakage caused by damage to the container. If leakage unfortunately occurs, quickly evacuate the irrelevant personnel and demarcate the warning area. Emergency responders must wear professional protective equipment, use appropriate materials to absorb and contain leaks, and dispose of them properly. They should not discharge them at will to avoid polluting the environment.
In short, the safe production and operation of diethyl oxalate is related to the safety of everyone and endangers the tranquility of the environment. It is necessary to carefully follow the regulations and not be slack.
Diethyl oxalate is one of the chemical products. To make this product, it is necessary to clarify its safety and operation specifications, so that it can be smooth and safe.
In the place of production, the first priority is safety. All facilities in the factory must be sturdy and intact, and the fire, explosion-proof and anti-virus equipment should be complete. When workers are working, they must wear special protective clothing, gas masks, goggles, etc., to prevent harm from contact with this product. In the workshop, ventilation must be good so that harmful gases can be discharged in time.
Its operation is also regulated. When feeding, the proportion and order of materials should not be wrong, and it should be done according to the precise formula. When reacting, the temperature and pressure must be strictly controlled, and a special person should be set up to monitor the number of instruments. If there is any abnormal movement, it should be disposed of immediately. The process of heating and cooling should also be done slowly and cannot be done.
Store diethyl oxalate, and also pay attention to it. It should be placed in a cool, dry and ventilated place, away from fire and heat sources. Do not mix with oxidants, acids and other substances to prevent chemical reactions and cause danger.
When handling, the action should be gentle, and it should not be loaded and unloaded savagely to avoid leakage caused by damage to the container. If leakage unfortunately occurs, quickly evacuate the irrelevant personnel and demarcate the warning area. Emergency responders must wear professional protective equipment, use appropriate materials to absorb and contain leaks, and dispose of them properly. They should not discharge them at will to avoid polluting the environment.
In short, the safe production and operation of diethyl oxalate is related to the safety of everyone and endangers the tranquility of the environment. It is necessary to carefully follow the regulations and not be slack.
Application Area
"On the application field of diethyl oxalate"
Diethyl oxalate is widely used in various fields. In the field of medicine, it is a key raw material for the synthesis of many drugs. It can use its unique chemical properties and subtle reaction paths to prepare drugs with specific curative effects and heal the world's diseases.
In the fragrance industry, it also plays an important role. Its participation in fragrance blending can add unique flavor to fragrances, make the aroma richer and more layered, and increase the charm and value of fragrances.
In the field of organic synthesis, diethyl oxalate is a common reagent. Helping organic chemists build complex molecular structures and open up new possibilities for organic synthesis is of great significance in chemical research and industrial production.
Diethyl oxalate is widely used in various fields. In the field of medicine, it is a key raw material for the synthesis of many drugs. It can use its unique chemical properties and subtle reaction paths to prepare drugs with specific curative effects and heal the world's diseases.
In the fragrance industry, it also plays an important role. Its participation in fragrance blending can add unique flavor to fragrances, make the aroma richer and more layered, and increase the charm and value of fragrances.
In the field of organic synthesis, diethyl oxalate is a common reagent. Helping organic chemists build complex molecular structures and open up new possibilities for organic synthesis is of great significance in chemical research and industrial production.
Research & Development
Taste the way of chemical industry, the most important lies in innovation, and it is related to the change of all things. Diethyl Oxalate is also diethyl oxalate, which is of great significance in the field of chemical industry.
We have dedicated ourselves to studying and exploring the method of its optimization. Looking at the way of its synthesis, trying new agents, adjusting temperature and pressure, hoping to improve the yield. After months of trial, some gains have been made. Under the new path, the yield is better than before, and the purity of the product is better.
However, the road of development has no end. Although it has achieved small success, it should still be unremitting. To explore its application widely, in the fields of medicine and materials, to expand its new territory. With continuous research, this product has become more and more prosperous in the industrial forest, contributing to the prosperity of the chemical industry and reaching a higher level.
We have dedicated ourselves to studying and exploring the method of its optimization. Looking at the way of its synthesis, trying new agents, adjusting temperature and pressure, hoping to improve the yield. After months of trial, some gains have been made. Under the new path, the yield is better than before, and the purity of the product is better.
However, the road of development has no end. Although it has achieved small success, it should still be unremitting. To explore its application widely, in the fields of medicine and materials, to expand its new territory. With continuous research, this product has become more and more prosperous in the industrial forest, contributing to the prosperity of the chemical industry and reaching a higher level.
Toxicity Research
"Study on the toxicity of diethyl oxalate"
There is now a chemical substance called diethyl oxalate (Diethyl Oxalate). We study its toxicity as the main point.
This substance has gradually shown its properties in various experiments. When entering the body of a white rat, at the beginning, the white rat moved a little slower, and then his diet gradually decreased. Looking at its physiology, there may be slight changes in the organs. For the liver, the color is slightly different, and its energy is also slightly reduced. The function of the kidneys is also in a state of fatigue.
Another plant was tried, and diethyl oxalate was applied to the seedlings. The growth of the seedlings was hindered, the leaves gradually wilted, and the stems were also weak.
In summary, diethyl oxalate is toxic and has adverse effects on animals and plants. The research results can be used for protection and protection to avoid its harm and ensure the well-being of all living beings.
There is now a chemical substance called diethyl oxalate (Diethyl Oxalate). We study its toxicity as the main point.
This substance has gradually shown its properties in various experiments. When entering the body of a white rat, at the beginning, the white rat moved a little slower, and then his diet gradually decreased. Looking at its physiology, there may be slight changes in the organs. For the liver, the color is slightly different, and its energy is also slightly reduced. The function of the kidneys is also in a state of fatigue.
Another plant was tried, and diethyl oxalate was applied to the seedlings. The growth of the seedlings was hindered, the leaves gradually wilted, and the stems were also weak.
In summary, diethyl oxalate is toxic and has adverse effects on animals and plants. The research results can be used for protection and protection to avoid its harm and ensure the well-being of all living beings.
Future Prospects
Diethyl Oxalate is also known as diethyl oxalate. In the field of chemical industry, it is widely used. Looking at its future development, it is really promising.
This substance is used in organic synthesis as an important raw material. In the future, science and technology will be new, and the method of organic synthesis will become more refined, and its demand will also increase. And it also has extraordinary effects in the medicine and fragrance industries. In the future, medicine will seek innovation and spices will seek differences. It depends on the help of this substance, and its market will become wider.
Although there may be difficulties ahead, such as strict environmental regulations and changes in raw material prices. However, those who are good at planning can turn difficulties into opportunities. With the power of science and technology, it can improve its productivity and reduce its energy consumption, which is in line with environmental protection regulations. Therefore, I believe that the future exhibition of Diethyl Oxalate will be like the rise of the sun, with a bright future, which can add brilliance to the chemical industry.
This substance is used in organic synthesis as an important raw material. In the future, science and technology will be new, and the method of organic synthesis will become more refined, and its demand will also increase. And it also has extraordinary effects in the medicine and fragrance industries. In the future, medicine will seek innovation and spices will seek differences. It depends on the help of this substance, and its market will become wider.
Although there may be difficulties ahead, such as strict environmental regulations and changes in raw material prices. However, those who are good at planning can turn difficulties into opportunities. With the power of science and technology, it can improve its productivity and reduce its energy consumption, which is in line with environmental protection regulations. Therefore, I believe that the future exhibition of Diethyl Oxalate will be like the rise of the sun, with a bright future, which can add brilliance to the chemical industry.
Where to Buy Diethyl Oxalate in China?
As a trusted Diethyl Oxalate manufacturer, we deliver:
Factory-Direct Value: Competitive pricing with no middleman markups, tailored for bulk orders and project-scale requirements.
Technical Excellence: Precision-engineered solutions backed by R&D expertise, from formulation to end-to-end delivery.
Whether you need industrial-grade quantities or specialized customizations, our team ensures reliability at every stage—from initial specification to post-delivery support.
As a leading Diethyl Oxalate supplier, we deliver high-quality products across diverse grades to meet evolving needs, empowering global customers with safe, efficient, and compliant chemical solutions.
What are the main uses of Diethyl Oxalate?
Diethyl oxalate (Diethyl Oxalate), this substance has a wide range of uses. In the process of chemical preparation, it is often used as an important raw material for organic synthesis. For example, in the pharmaceutical field, it can provide a key starting material for the synthesis of many drugs. Because its structure contains specific functional groups, it can be converted into structural fragments required by drug molecules through various chemical reactions.
In the fragrance industry, it also has its uses. It can be used to participate in the reaction to generate compounds with unique aromas, and added to the fragrance formula to give the fragrance a different flavor and increase its aroma richness and uniqueness.
Furthermore, in the production of plastic additives, diethyl oxalate also plays an important role. It can be processed by a specific process to prepare additives with good compatibility with plastics, improve the properties of plastics, such as improving their flexibility and stability, etc., so that the quality of plastic products is better and the application scenarios are wider.
And in organic synthetic chemistry experiments, diethyl oxalate is a common reagent. Researchers use it to participate in various reactions, explore new synthesis routes, expand the types of organic compounds, and promote the development of organic chemistry. In short, diethyl oxalate plays an indispensable role in many industrial and scientific research fields, with diverse and critical uses.
What are the physical properties of Diethyl Oxalate?
Diethyl oxalate (Diethyl Oxalate) is an organic compound. Its physical properties can be described in many ways.
Looking at its properties, it is a colorless oily liquid under normal circumstances, clear and transparent, flowing like jade liquid. Its taste is fragrant, slightly prickly, and can be detected in the air.
When it comes to the melting point, it is about -40.6 ° C. If it drops to Swain, the liquid gradually condenses and turns into a solid state, but its solidified state does not lose its crystal quality. The boiling point is 185.4 ° C. When the temperature rises to this point, the liquid tumbles and turns into steam.
Its density is about 1.0785 (g/cm ³), which is slightly heavier than water. If it is placed in water, it will slowly sink to the bottom, like the sinking beads of water. And it is mutually soluble with most organic solvents, such as ethanol and ether. When it blends, it is like water and milk, regardless of each other.
And because of its volatility, it is left in the air for a long time, and its amount is gradually reduced, such as the dissipation of mist. The vapor of this substance is heavier than air, and can spread along the ground and accumulate in low-lying places.
In terms of solubility, it is slightly soluble in water. If it is estranged in water, it can only be dispersed in a small amount, and it is difficult to form a whole.
Diethyl oxalate has unique physical properties and is useful in many fields such as chemical industry and medicine. It is effective due to its characteristics and adds color to various processes.
What are the chemical properties of Diethyl Oxalate?
Diethyl oxalate, its chemical properties are quite characteristic. This is a colorless oily liquid with a fragrant smell.
In terms of its chemical properties, hydrolysis is remarkable. In acidic media, diethyl oxalate can slowly hydrolyze to form oxalic acid and ethanol. This hydrolysis process is gradual, and the ester group of diethyl oxalate is gradually broken by hydrogen ions, so this change occurs. In alkaline media, the hydrolysis rate is accelerated, and the reaction is more rapid, resulting in oxalate and ethanol. This basic hydrolysis reaction is often used in organic synthesis as a way to prepare oxalates.
Furthermore, diethyl oxalate has the ability to esterify. It can react with alcohols under acid catalysis to form new ester compounds. This reaction enhances the positive electricity of carbonyl carbon through acid catalysts, making the nucleophilic attack of alcohols more likely to occur, thereby realizing the conversion of ester groups and the formation of new esters.
In addition, diethyl oxalate can also participate in the condensation reaction. Under the action of strong bases, the α-hydrogen of diethyl oxalate can be removed to generate carbon negative ions. This carbon negative ion has high activity and can condensate with other carbonyl-containing compounds to form carbon-carbon bonds. It is widely used in the field of complex molecular construction in organic synthesis.
And diethyl oxalate can be reduced. Under the action of suitable reducing agents, its ester groups can be reduced to alcohol hydroxyl groups to obtain products such as ethylene glycol. This reduction reaction provides an effective path for the preparation of specific alcohols.
The chemical properties of diethyl oxalate play important functions in many fields such as organic synthesis, drug preparation, and fragrance production, and contribute greatly to the development of the chemical industry.
What are the production methods of Diethyl Oxalate?
Diethyl oxalate is an organic compound. There are several common methods for its preparation:
First, oxalic acid and ethanol are used as raw materials for esterification. This reaction needs to be carried out at a suitable temperature and in the presence of a catalyst. Mix oxalic acid with ethanol, add a catalyst such as sulfuric acid, and heat it to react. Sulfuric acid can promote the reaction to form diethyl oxalate. After the reaction is completed, the sulfuric acid needs to be properly treated to remove impurities. The reaction formula is: $H_ {2} C_ {2} O_ {4} + 2C_ {2} H_ {5} OH\ xrightarrow [] {H_ {2} SO_ {4},\ Delta} (C_ {2} H_ {5} O) _ {2} C_ {2} O_ {4} + 2H_ {2} O $.
Second, ethyl chloroacetate is used as raw material and obtained by cyanidation, hydrolysis and esterification. First, ethyl chloroacetate is reacted with sodium cyanide to obtain ethyl cyanoacetate. This step needs to pay attention to the reaction conditions to prevent cyanide from escaping. Ethyl cyanoacetate is then hydrolyzed to form a sodium salt of monoethyl oxalate, then acidified to obtain monoethyl oxalate, and finally esterified with ethanol to obtain diethyl oxalate. The series of reactions is quite complicated, and each step requires precise temperature control and reaction process.
Third, carbon monoxide, ethanol and oxygen are used as raw materials and synthesized under the action of catalysts. This is a relatively novel method, which requires a specific catalyst system, such as metals such as palladium as active components. The raw materials of this method are easy to obtain, but the requirements for reaction equipment and conditions are quite high. Under certain pressure and temperature, carbon monoxide, ethanol and oxygen are reacted on the surface of the catalyst to form diethyl oxalate.
All preparation methods have advantages and disadvantages. In actual production, it is necessary to comprehensively weigh factors such as raw material availability, cost, and product purity to choose the optimal method.
What are the precautions for using Diethyl Oxalate?
Diethyl oxalate (Diethyl Oxalate), the raw material of chemical, is widely used in various fields of industry. When it is used, several things should be paid attention to.
First, it is related to safety. Diethyl oxalate is flammable. When used in places, open flames and heat must be avoided to prevent the risk of fire and explosion. And it has irritation to people, skin, eye contact, or discomfort. When operating, protective equipment, such as gloves and goggles, should be prepared, and the ventilation of the field must be good, so that the gas is concentrated and the poison is avoided.
Second, on storage. It should be stored in cool, dry, and ventilated storage, away from fire and heat sources. The storage area should be equipped with suitable containment materials for leakage emergency departments. It should not be stored in combination with oxygen agents and alkalis, etc., to prevent chemical and life risks.
Third, it involves the use of technology. Operators should be specially trained and abide by regulations. When taking it, the quantity should be precisely controlled to avoid waves and overuse. And in the chemical application, temperature, pressure, time and other conditions should be strictly monitored and adjusted to ensure that it should be carried out smoothly, and the quality and rate of production are guaranteed.
Fourth, talk about waste. Diethyl oxalate is used up, and it should not be discarded indiscriminately. Dispose of it according to ring regulations. Or recycle it, or deal with it through special treatment methods, so that it is harmless to the ring.
In short, when diethyl oxalate is used, safety, storage, technology, and waste should be paid attention to, so as to ensure smooth use, avoid risks, and protect people's safety and environmental health.
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